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CAT NO: DIDACTICChemical Engineering0017
Emulsion Polymerization Reactor.
Emulsion Polymerization Reactor
The set-up consists of jacketed type SS reactor fitted with a
variable speed agitator and baffles.
Hot water from a digitally
controlled water bath is circulated in the jacket using a pump. Metered
quantity of nitrogen gas from a cylinder passes through a de-oxygenation
column & allowed to enter in the reactor. Air has to be evacuated
using a vacuum pump to create vacuum up to 30mm of Hg before passing the
nitrogen supply. Initiator from reservoir is supplied to the reactor
under pressure. Set-up is complete& self-contained with sampling
ports.
Experiments
Effect of monomer concentration
Effect of Initiator concentration.
Effect of emulsifier concentration.
Effect of RPM on conversion
Utilities Required
Water supply and drain.
Electricity- 1.5kw, Single.
Instruments, Laboratory wares and Chemicals required for analysis as per the system adopted.
Vacuum Pump
High purity N2 gas
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