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CAT NO: DIDACTICChemical Engineering0018
Condensation Polymerization Reactor.
Condensation Polymerization Reactor
Condensation Polymerization kettle is used to carry out a
condensation polymerization reaction under batch condition.
Polymerization reaction can be acid catalyzed or self-catalyzed.
The
set-up can be used to measure the extent of reaction &.also the
reaction rate constant. The set-up consists of jacketed type SS reactor
fitted with variable speed agitator & baffles. Reactor is fitted
with Nichrome wire heaters and digital temperature controller controls
temperature. Metered quantity of nitrogen gas from a cylinder, allowed
entering, in the reactor. Set-up is complete &. self-contained with
sampling ports. The top cover can be removed for cleaning purpose. Feed
is fed from top through a funnel provided with S.S. Ball Valve. An
outlet is given to Condenser fitted with a Perken's triangle for
collecting the condensate. Vapors are allowed to enter in the shell of
condenser and cooling water is allowed to pass through the tube and
condensate is collected.
Experiments
To determine
the kinetic parameters of a Condensation polymerization reaction between
Pthalic acid and Hexamethylene diamine with &.without acid catalyst
Utilities Required
Water supply and drain
Electricity-I.5kw, Single
Space 0.7m x 0.7m x 1.0m
Instruments, Laboratory wares and Chemicals required for analysis as per the system adopted.
High purity N2 gas
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